TripleXtacy (Stranger)
09-19-01 10:01
No 215063
      Aniline synth???  Bookmark   

A friend of swims who likes to play with fentanyl, has recently encountered a stumbling block. Due to new obstacles recently imposed in his area in regards to acquisitions of aniline have led him to discover new methods of possession.
His question is, has anyone experimented with the production of aniline via hydrogenation of nytrobenzene with Iron turnings/fillings?
If not has anyone got any tips as he is ready to give it a try anyways.
Thanks for your time.

The only secrets are the ones that keep themselves.
 
 
 
 
    Rhodium
(Chief Bee)
09-19-01 10:06
No 215065
      Re: Aniline synth???  Bookmark   

Yes, and it is an easy reduction. Look in the file ../rhodium/chemistry /quaalude.txt for general directions.
 
 
 
 
    Bwiti
(PVC-Analog Taste-Tester)
06-05-02 01:41
No 317655
      That text doc was HTMLized to http://www.rhodium.  Bookmark   

That text doc was HTMLized to ../rhodium/chemistry /quaalude.cheapskate.htmlcool

Love my country, fear my government.
 
 
 
 
    Rhodium
(Chief Bee)
06-05-02 01:46
No 317657
      Yup, 300 documents HTMLized so far, 100 to go.  Bookmark   

Yup, 300 documents HTMLized so far, 100 to go.
 
 
 
 
    PrimoPyro
(Hive Prodigy)
06-05-02 01:49
No 317659
      Aniline  Bookmark   

Can also be made by reaction of benzamide with hypochlorite salts. Another easy reaction, and Cheapskate used the same principle for his Anthranilic acid synthesis, from phthalic acid.

                                                    PrimoPyro
 
 
 
 
    PolytheneSam
(Master Searcher)
06-05-02 03:15
No 317682
      From what I remember the process in J. Gen. Chem.  Bookmark   

From what I remember the process in J. Gen. Chem. is electrochemical.  Post 199874 (PolytheneSam: "Re: Oxidative amination of an alkene, maybe an electro possiblity.", Chemistry Discourse)

http://www.geocities.com/dritte123/PSPF.html
The hardest thing to explain is the obvious
 
 
 
 
    hellman
(Stranger)
06-19-02 03:10
No 322878
      very easy  Bookmark   

Benzene-nitrobenzene`````h2so4
nitrobenzene-anilin''''''zn/hcl or sn/hcl
If you want the procedure step by step just ask,.
It is also from vogels pract