synthesys (Stranger)
03-18-03 20:38
No 418708
      NH2OH + MDP2P -> R'N-OH +GAA+ Pd/C+H2 -> ?  Bookmark   

If you hydrogented an oxime of NH2OH/MDP2P, and the resulting oil had most of the properties of MDA freebase, but was not soluble in acidic water, then the reduction was not complete, than you have something like RNHOH instead of RNH2. How can I determine that? If it proves to be RNHOH, can I use NaBH4 to reduce it further?

(Hive Addict)
03-19-03 03:30
No 418879
      Fuck all that  Bookmark   

reduce the oxime with aa/al/hg.  search anitbodys posts.  80%yeild

Start thinking more like a chemist and less like a criminal