|Concise Large -scale synthesis of Psilocybin and..||Bookmark|
Concise Large-Scale Synthesis of Psilocin and Psilocybin, Principal Hallucinogenic Constituents of "Magic Mushroom"
Osamu Shirota, Wataru Hakamata, and Yukihiro Goda
J. Nat. Prod.; 2003; ASAP Web Release Date: 30-May-2003;
(Note) DOI: 10.1021/np030059u
We're all in this world together,
Large-scale syntheses of Psilocin/Psilocybin
(Rated as: excellent)
Java: I've found that article at about the same time as you did, just saw it! Amazing... Amazing...
However, here is the full-text for those without acsess: http://pharmacist8.tripod.com/psiloindus
Abstract: The concise large-scale syntheses of psilocin (1) and psilocybin (2), the principal hallucinogenic constituents of "magic mushroom", were achieved without chromatographic purification. The key step in the synthesis of 2 was the isolation of the dibenzyl-protected intermediate (7) as a zwitterionic derivative (8), which was completely identified by means of 2D NMR analyses.
This is major advance when it comes to synth of psilocybin considering the shitty yield (10%) as presented in TiHKAL for the preparation of the phosphate ester...
Accept No Imitations, There Can Only Bee One; www.the-hive.ws
|Already at my page||Bookmark|
I have uploaded it to ../rhodium/pdf /psilocin-psil